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SCI Article

Pd nanoparticles on reverse phase silica gel as recyclable catalyst for Suzuki-Miyaura cross couplin
Author Lee, Sinyoung (Dept Bionanotechnol); Lim, Minkyung (Dept Bionanotechnol); Lee, Heejin (Dept Bionanotechnol); Lee, Youngbok (Dept Bionanotechnol); Rhee, Hakjune (Dept Bionanotechnol); Shabbir, Saira (Dept Appl Chem); Ko, Hyeji (Dept Appl Chem); Lee, Young
Corresponding Author Info Rhee, H (reprint author), Hanyang Univ, Dept Bionanotechnol, Hanyang Daehak Ro 55, Ansan 15588, Gyeonggi Do, South Korea.
E-mail 메일hrhee@hanyang.ac.kr
Document Type Article
Source JOURNAL OF ORGANOMETALLIC CHEMISTRY Volume:846 Issue: Pages:296-304 Published:2017
Times Cited 0
External Information pdfhttp://dx.doi.org/10.1016/j.jorganchem.2017.07.003
Abstract Two catalytic systems, consisting of palladium nanoparticles supported by reverse phase amino functionalized silica are utilized as catalysts for Suzuki-Miyaura reaction and hydrogenation in water. The catalysts were developed by modifying silica into bidentate ligands, using either 2-pyridinecarboxaldehyde or 2,2'-bipyridine-4,4'-dicarboxylic acid. The synthesized catalysts showed quantitative reaction yields and recyclability with negligible leaching of Pd nanoparticles. Various characterization techniques including XPS, ICP-MS, SEM, BET, XRD, TEM, H-1-and C-13-NMR are used to verify the efficiency of the catalysts. (C) 2017 Elsevier B.V. All rights reserved.
Web of Science Categories Chemistry, Inorganic & Nuclear; Chemistry, Organic
Funding Basic Science Research Program through the National Research Foundation of Korea (NRF); Ministry of Education [2015R1D1A1A09058536]; Korean Ministry of Education through the BK21-Plus Project of the Hanyang University Graduate Program
Language English
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